Flexible and free-standing films containing cobalt-doped nanocrystalline zinc oxide dispersed in polyvinylidene fluoride matrix: synthesis and characterization
| Autor: | Ritamay Bhunia, Arun Kumar Pal, Sajjad Hussain, Radhaballav Bhar, Bibhash Ranjan Chakraborty, Rajkumar Dey |
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| Rok vydání: | 2017 |
| Předmět: |
Materials science
Polymers and Plastics Composite number Analytical chemistry chemistry.chemical_element 02 engineering and technology 010402 general chemistry 01 natural sciences chemistry.chemical_compound symbols.namesake X-ray photoelectron spectroscopy Materials Chemistry Doping General Chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics Polyvinylidene fluoride Nanocrystalline material 0104 chemical sciences Secondary ion mass spectrometry Chemical engineering chemistry symbols 0210 nano-technology Raman spectroscopy Cobalt |
| Zdroj: | Polymer Bulletin. 75:307-325 |
| ISSN: | 1436-2449 0170-0839 |
| DOI: | 10.1007/s00289-017-2032-0 |
| Popis: | Synthesis of free-standing flexible Co-ZnO/PVDF composite films is realized by sol–gel technique. Modulation of the optical and microstructural properties of the above composite films with Co-doped nanocrystalline ZnO loading in PVDF matrix was studied critically. Uniform dispersion of Co-doped ZnO in PVDF matrix was indicated by SIMS studies. Information on the bonding environment was obtained from X-ray photoelectron spectroscopy and Raman spectroscopy studies. A very strong peak at ~695 eV for core level spectra of F1s along with those for C1s, Zn2p and Co2p dominated the XPS spectra of the composite films. Presence of the predominant β-phase of PVDF along with peaks related to ZnO nanocrystals in the poled sample was observed in the Raman spectra. |
| Databáze: | OpenAIRE |
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