Electron microscopy of ultra-thin buried layers in InP and InGaAs

Autor: M.R. Aylett, Nikolaus Grigorieff, M.J. Yates, D. Cherns, S.D. Perrin, M. Hockly
Rok vydání: 1993
Předmět:
Zdroj: Philosophical Magazine A. 68:121-136
ISSN: 1460-6992
0141-8610
DOI: 10.1080/01418619308219361
Popis: The large-angle convergent-beam electron diffraction (LACBED) technique has been used to measure layer thicknesses and strain of ultra-thin arsenic and phosphorus-rich layers produced by temporary arsine and phosphine purges in the metal-organic vapour phase epitaxy growth of InP and InGaAs. The paper describes how the technique, previously used to investigate single quantum wells of thickness between 8 and 30 A, has been extended to layers of thicknesses of one to two monolayers. It is shown that LACBED patterns can be recorded under conditions in which only a small constant inelastic background and elastic scattering need be considered and can be analysed in detail using a kinematical approach. By combining LACBED results with dark-field images showing the presence of interfacial steps and high-resolution images from cross-sectional samples, a more detailed understanding of the growth interrupt layers is derived.
Databáze: OpenAIRE