Studying surfaces and thin films using Mössbauer spectroscopy

Autor: Laura K. Perry, D. H. Ryan, R. Gagnon
Rok vydání: 2006
Předmět:
Zdroj: Hyperfine Interactions. 170:131-143
ISSN: 1572-9540
0304-3843
Popis: Using a series of bi-layer samples, we show how Conversion Electron Mossbauer Spectroscopy (CEMS) and X-ray Backscatter Mossbauer Spectroscopy (XBS) can be done with the same experimental set up. The penetration depths of the K and L conversion electrons are measured as 51(6) and 330(240) nm, respectively, with relative contributions of 88(9) and 12(9)%. The penetration depth of the Fe-K α X-ray signal is determined to be 3.6(2) μm. As a demonstration we show data on surface damage effects in electropolished TRIP steels, and by comparing CEMS and XBS Mossbauer patterns we estimate the thickness of a damaged layer (created by sanding) to be 550(50) nm.
Databáze: OpenAIRE