Synthesis and crystal structure of a Pb complex with ciprofloxacin

Autor:	Liang-Cai Yu, H. M. Peng
Rok vydání:	2012
Předmět:	Crystallography Chemistry Elemental analysis General Chemical Engineering Hydrothermal reaction General Chemistry Trigonal crystal system Crystal structure Single Crystal Diffraction
Zdroj:	Russian Journal of Coordination Chemistry. 38:392-395
ISSN:	1608-3318 1070-3284
DOI:	10.1134/s1070328412060115
Popis:	A hydrothermal reaction of ciprofloxacin with PbCl2 · 2H2O and Na2S yields a metal complex [Pb2(H-Cip)6S]Cl6 (I), which was characterized by elemental analysis, IR, and single crystal diffraction analyses. Complex I crystallizes in the rhombohedral system, space group \(R\bar 3c\), with lattice parameters a = 15.7800(7), c = 77.901(9) A, V = 16799(2) A3, Z = 12, ρcalcd = 1.646 mg/m3.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::645cdfd6115733a1d56e1a0deb24d388 https://doi.org/10.1134/s1070328412060115 Zobrazit plný text záznamu Full text from SpringerLink