An Investigation of Facile One-Pot Synthesis of Li2FeSiO4/C Composite for Li Ion Batteries
| Autor: | Hariharan Kaluvan, Mani Chandran Thirumoolam, Balaji Sivaramakrishnan, Mohan Rao Gowravaram, Ananda Kumar Manikandan |
|---|---|
| Rok vydání: | 2017 |
| Předmět: |
Materials science
Composite number 02 engineering and technology 010402 general chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics Combustion 01 natural sciences Electron spectroscopy 0104 chemical sciences Electronic Optical and Magnetic Materials Amorphous solid Dielectric spectroscopy chemistry.chemical_compound Lattice constant chemistry Materials Chemistry Urea Orthorhombic crystal system Electrical and Electronic Engineering 0210 nano-technology Nuclear chemistry |
| Zdroj: | Journal of Electronic Materials. 47:1952-1961 |
| ISSN: | 1543-186X 0361-5235 |
| DOI: | 10.1007/s11664-017-5996-5 |
| Popis: | Li2FeSiO4 and its carbon composite are prepared by an urea-assisted combustion method. The synthesis has been carried out in different urea concentrations, namely 1 Molar (M), 2 M and 3 M urea in the cost-effective ambient atmospheric condition. The x-ray diffraction analysis confirms the orthorhombic structure of Li2FeSiO4 compounds. The urea-assisted combustion reaction enhanced the phase purity of the compound and prevented the oxidation of ferrous ions in Li2FeSiO4. The x-ray photo electron spectroscopy analysis further confirmed the reduction of Fe3+ concentration in Li2FeSiO4 while adding urea. The Li2FeSiO4 compound formation in the presence of urea occurred at a temperature |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|
Full text from SpringerLink