Chromone studies. Part 3. NMR analysis of rotational isomerism in 4-oxo-4H-chromene-2-carboxamides

Autor: Deborah N. Davidson, Perry T. Kaye
Rok vydání: 1991
Předmět:
Zdroj: Journal of the Chemical Society, Perkin Transactions 2. :927
ISSN: 1364-5471
0300-9580
DOI: 10.1039/p29910000927
Popis: Temperature dependent splitting of N-alkyl 1H and 13C NMR signals in a series of 4-oxo-4H-chromene-2-carboxamides has been analysed in terms of rotation of the amide group. Rotational barriers have been calculated from dynamic 1H NMR data and the conformational options have been explored.
Databáze: OpenAIRE