Novel Bis[N-alkyl-N-(2-diphenylphosphinylethyl)]diglycolamides: Synthesis and NMR Spectroscopy Studies

Autor:	N. A. Bondarenko, K. V. Tcarkova, S. K. Belus, Alexander S. Peregudov, Oleg I. Artyushin
Rok vydání:	2021
Předmět:	Phosphine oxide chemistry.chemical_classification Primary (chemistry) Aqueous solution 010405 organic chemistry General Chemistry Nuclear magnetic resonance spectroscopy 010402 general chemistry Alkali metal 01 natural sciences Medicinal chemistry Chloride 0104 chemical sciences chemistry.chemical_compound chemistry medicine 31p nmr spectroscopy Alkyl medicine.drug
Zdroj:	Russian Journal of General Chemistry. 91:181-189
ISSN:	1608-3350 1070-3632
DOI:	10.1134/s1070363221020055
Popis:	Pentadentate bis[N-alkyl-N-(2-diphenylphosphinylethyl)]diglycolamides [Ph2P(O)CH2CH2N(R)· C(O)CH2]2O, where R Me, Bu, Oct, were synthesized by reaction of diglycolyl chloride with N-alkyl-N-(2-diphenylphosphinylethyl)amines Ph2P(O)CH2CH2NHR obtained by reacting diphenyl(2-phenoxyethyl)phosphine oxide with primary alkylamines in DMSO in the presence of an aqueous alkali. Structure of the prepared compounds was studied by 1H, 13C, and 31P NMR spectroscopy.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::6154ea4ba119c4d9cfa468e1713e3fad https://doi.org/10.1134/s1070363221020055 Zobrazit plný text záznamu Plný text ve formátu PDF Plný text ve formátu HTML
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