Two-stage synthesis of ultrafine powder of chromium carbide
Autor: | I. V. Nikolaenko, Gennadii Shveikin, Svetlana Antipina |
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Rok vydání: | 2017 |
Předmět: |
010302 applied physics
Materials science Chromium Compounds Precipitation (chemistry) Carbonization Thermal decomposition Metallurgy Metals and Alloys chemistry.chemical_element 02 engineering and technology 021001 nanoscience & nanotechnology Condensed Matter Physics 01 natural sciences Carbide chemistry.chemical_compound Chromium chemistry Specific surface area 0103 physical sciences Materials Chemistry Physical and Theoretical Chemistry 0210 nano-technology Chromium carbide |
Zdroj: | International Journal of Materials Research. 109:83-86 |
ISSN: | 2195-8556 1862-5282 |
DOI: | 10.3139/146.111577 |
Popis: | A new method for the synthesis of ultrafine powder of chromium carbide is proposed, which combines liquid-phase precipitation on a carbon support and low-temperature microwave heat treatment in argon flow. The whole spectrum of the intermediate compounds obtained during thermolysis, reduction and carbonization of chromium precursors to the final product Cr3C2 is presented. The structure, morphology, particle size distribution, as well as the phase composition and the specific surface area values of the produced chromium compounds are shown. |
Databáze: | OpenAIRE |
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