Synthesis and characterization of hydroxyapatite nanoparticles templated by ozonolysed natural rubber latex
| Autor: | Songkot Utara, Jutharatana Klinkaewnarong |
|---|---|
| Rok vydání: | 2016 |
| Předmět: |
Materials science
Nanoparticle 02 engineering and technology 010402 general chemistry 01 natural sciences Biomaterials Crystallinity Differential scanning calorimetry stomatognathic system Natural rubber Polymer chemistry Materials Chemistry Hydroxyapatites Fourier transform infrared spectroscopy General Chemistry 021001 nanoscience & nanotechnology Condensed Matter Physics 0104 chemical sciences Electronic Optical and Magnetic Materials Thermogravimetry Chemical engineering Transmission electron microscopy visual_art Ceramics and Composites visual_art.visual_art_medium sense organs 0210 nano-technology |
| Zdroj: | Journal of Sol-Gel Science and Technology. 80:728-737 |
| ISSN: | 1573-4846 0928-0707 |
| DOI: | 10.1007/s10971-016-4171-4 |
| Popis: | Nanoscale hydroxyapatites (HAps) were successfully synthesized by means of sol–gel method in the presence of ozonolysed natural rubber latex templates of various molecular weights. The thermal properties, functionality, crystallinity and morphology of HAp powder were characterized by simultaneous thermogravimetry and differential scanning calorimetry, Fourier transform infrared spectroscopy, X-ray diffraction and transmission electron microscopy. The results revealed that lower molecular weight ozonolysed natural rubber templates produced spheroidal and less crystalline HAp nanoparticles. A higher molecular weight template produced HAp nano-rod-like particles with higher crystallinity. The results obtained in this work suggest that the molecular weight as well as functionality of the biomacromolecule template affect the phase crystallinity and morphology of synthesized HAp. |
| Databáze: | OpenAIRE |
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