Chlorotrimethylsilane-Promoted Synthesis of 1,2-Dihydro-1-Arylnaphtho [1,2-e] [1,3]Oxazine-3-Ones

Autor: Chenggang Jiang, Xin Geng, Cunde Wang, Zonglei Zhang, Hangxian Xu
Rok vydání: 2010
Předmět:
Zdroj: Journal of Chemical Research. 34:19-21
ISSN: 2047-6507
1747-5198
Popis: Chlorotrimethylsilane (TMSCI) is effective as a catalyst for the preparation of 1,2-dihydro-1-arylnaphtho[1,2-e] [1,3]oxazine-3- ones using a one-pot condensation of 2-naphthol, aromatic aldehydes and urea in DMF as solvent. The reaction times, temperature, and catalyst amounts were varied.
Databáze: OpenAIRE