Continuous-Flow Synthesis of Functional Carbonaceous Particles from Biomass under Hydrothermal Carbonization
Autor: | Dong-Pyo Kim, Seungwook Jang, Ajay Singh, Yun Zhao, Anjie Wang |
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Rok vydání: | 2014 |
Předmět: | |
Zdroj: | Journal of Flow Chemistry. 4:195-199 |
ISSN: | 2063-0212 2062-249X |
Popis: | Plain and N-doped carbonaceous particles are synthesized from biomass resources such as glucose via continuous hydrothermal carbonization (HTC) process at 200 °C and 250 psi for the first time using a microfluidic system in a fast and continuous manner. The continuous HTC is controlled by reaction time (3.7–30 min) and concentration (0–10 wt.%) of ethylenediamine as a nitrogen additive to produce a series of the plain carbonaceous and N-doped carbonaceous particles with size range from 0.8 to 1.2 um. The as-synthesized and the pyrolyzed particles are characterized by various analytical instruments to understand their chemical structures with elemental compositions, morphology of particles, and thermal defunctionalization. |
Databáze: | OpenAIRE |
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