ChemInform Abstract: Vilsmeier Reagents: Preparation of β-Halo α,β-Unsaturated Ketones

Autor: Richard E. Mewshaw
Rok vydání: 1990
Předmět:
Zdroj: ChemInform. 21
ISSN: 0931-7597
DOI: 10.1002/chin.199008087
Popis: A new method for the preparation of β-chloro and β-bromo-α,β-unsaturated ketones from β-diketones is described. Utilizing Vilsmeier reagents (prepared from N,N-dimethylformamide and oxalyl chloride or oxalyl bromide) β-halo-α,β-unsaturated ketones are isolated in excellent yields.
Databáze: OpenAIRE