Synthesis and NMR Characterization of Monomethoxypoly(Ethylene Glycol) Aldehydes from Monomethoxypoly(Ethylene Glycol) Tosylates

Autor: David L. Ladd, P. Mark Henrichs
Rok vydání: 1998
Předmět:
Zdroj: Synthetic Communications. 28:4143-4149
ISSN: 1532-2432
0039-7911
Popis: A procedure for the synthesis of monomethoxypoly(ethylene glycol) aldehydes from monomethoxypoly(ethylene glycol) tosylates is described. The tosylates are converted to aldehydes in high yield via treatment with disodium hydrogen phosphate and DMSO; minimal oligomeric by-products are formed.
Databáze: OpenAIRE