Comparison of supercritical fluid extraction and Soxhlet extraction of organic compounds from carpet samples

Autor:	James R. Bowyer, Joachim D. Pleil
Rok vydání:	1997
Předmět:	Chromatography Chemistry Organic Chemistry Extraction (chemistry) Supercritical fluid extraction Analytical chemistry General Medicine Environmental exposure Mass spectrometry Biochemistry Analytical Chemistry Benzene derivatives Extraction methods Gas chromatography
Zdroj:	Journal of Chromatography A. 787:171-179
ISSN:	0021-9673
DOI:	10.1016/s0021-9673(97)00624-9
Popis:	Supercritical fluid extraction (SFE) and Soxhlet extraction were applied to a common set of samples to determine their relative efficiencies for the measurement of a variety of organic compounds and their comparability as laboratory techniques. For this test, a variety of carpet samples were extracted by both SFE and Soxhlet methods and the extraction solutions were analyzed via gas chromatography/mass spectrometry. The results relative to an internal standard spike were then compared statistically by their relative standard deviations, an F-test for precision, and their averages within a 95% confidence level. Compounds of possible environmental exposure concern were used as some of the selected compounds for comparison.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::522d819d9fe03acb1e428fd54b3049d2 https://doi.org/10.1016/s0021-9673(97)00624-9 Zobrazit plný text záznamu Full Text from ScienceDirect