Features of Preparation of Multilayer Ultrathin Coatings from Thermosetting Epoxy Amine Systems by Spin-Coating Technique
Autor: | V. A. Zakharova, I. N. Senchikhin, A. V. Zaitseva, E. S. Zhavoronok, T. V. Kharitonova |
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Rok vydání: | 2020 |
Předmět: |
Spin coating
Materials science 010304 chemical physics Silicon Thermosetting polymer chemistry.chemical_element 02 engineering and technology Surfaces and Interfaces Epoxy engineering.material 021001 nanoscience & nanotechnology 01 natural sciences Surface energy Colloid and Surface Chemistry Coating chemistry visual_art 0103 physical sciences visual_art.visual_art_medium engineering Amine gas treating Physical and Theoretical Chemistry Thin film Composite material 0210 nano-technology |
Zdroj: | Colloid Journal. 82:584-591 |
ISSN: | 1608-3067 1061-933X |
Popis: | The basic factors influencing the quality of thin films prepared by the spin-coating technique from thermosetting stoichiometric epoxy-amine mixtures have been studied. It has been shown that films 2.5–3.0 nm thick are formed on silicon supports from a 0.025 wt % solution of the stoichiometric mixture of epoxy resin and amine in toluene. Multilayer polymer coatings with thickness up to 40 nm have been prepared from successively deposited partially cured epoxy-amine layers. The thickness of these coatings grows linearly with an increase in the number of layers, while their surface energy decreases. The revealed features may be used for creating multilayer polymer coatings, the properties of which vary along the coating thickness. |
Databáze: | OpenAIRE |
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