New Sulfamides Based on 1-Izopropil-3-α-Naftyl-5- Methoxymethyl-4-Aminopyrazole and Determination of Their Structure

Autor:	Ilya G. Povarov, Alexey V. Lubyashkin, Ekaterina V. Neupokoeva, G. A. Suboch, Nikita A. Shilenkov, Ivan V. Peterson, Mikhail S. Tovbis
Rok vydání:	2019
Předmět:	chemistry.chemical_classification chemistry General Chemical Engineering Proton NMR Infrared spectroscopy General Chemistry Mass spectrometry Sulfonamide Nuclear chemistry
Zdroj:	Journal of Siberian Federal University. Chemistry. :405-412
ISSN:	2313-6049 1998-2836
DOI:	10.17516/1998-2836-0137
Popis:	For the previously obtained 1-isopropyl-3-α-naphthyl-5-methoxymethyl-4-nitrosopyrazole, a reduction reaction with hydrazine hydrate was performed. It was first synthesized by 1-isopropyl-3-α-naphthyl- 5-methoxymethyl-4-aminopyrazole which was then sulfonylated by p-acetamidobenzenesulfonyl chloride and p-toluenesulfonic chloride. As a result previously unknown sulfonylated derivatives of N-alkylated aminopyrazoles were obtained. The composition and structure are confirmed by modern methods of analysis such as IR, 1H NMR spectroscopy and mass spectrometry
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::51a93122a5d09e5ae047c992501db1a7 https://doi.org/10.17516/1998-2836-0137 Zobrazit plný text záznamu