Rapid determination of 239,240Pu, 238Pu, 241Am and 90Sr in high contaminated samples waste using combined SPE sorbents AnaLig® Pu-02, AnaLig® Sr-01 and DGA® Resin
Autor: | Igor Antalík, Andrej Mátel, Boris Remenec, Miroslav Labaška, Silvia Dulanská |
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Rok vydání: | 2012 |
Předmět: |
Strontium
Chromatography Materials science Health Toxicology and Mutagenesis Public Health Environmental and Occupational Health Alpha-particle spectroscopy chemistry.chemical_element Americium Contamination Pollution Isotopes of strontium Analytical Chemistry Plutonium Matrix (chemical analysis) Cartridge Nuclear Energy and Engineering chemistry Radiology Nuclear Medicine and imaging Spectroscopy |
Zdroj: | Journal of Radioanalytical and Nuclear Chemistry. 295:1635-1639 |
ISSN: | 1588-2780 0236-5731 |
DOI: | 10.1007/s10967-012-2174-3 |
Popis: | A rapid separation method has been developed which allows measurement of plutonium, americium and strontium isotopes in the high active sample from CBRN Training and Testing Centre in Zemianske Kostolany (Slovakia) with high chemical recoveries and effective removal of matrix interferences. This method uses different commercial products stacked AnaLig® Pu-02, AnaLig® Sr-01 and DGA® Resin cartridges from IBC Advanced Technologies and Eichrom Technologies. The method allows rapid separation of plutonium, strontium and americium using a single multi-stage column in the vacuum box (cartridge technology) with rapid flow rates to minimize sample separation time. The 239,240Pu, 238Pu and 241Am were determined by alpha spectroscopy, 90Sr was counted on TRICARB 2900 TR by Cerenkov counting of its progeny 90Y. |
Databáze: | OpenAIRE |
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