The wet oxidation of bone Digestion with 100 per cent sulphuric acid followed by the addition of dioxonium perchlorate

Autor: Harvey Diehl, G. Frederick Smith
Rok vydání: 1959
Předmět:
Zdroj: Talanta. 3:41-46
ISSN: 0039-9140
DOI: 10.1016/0039-9140(59)80169-7
Popis: Organic materials rich in fat, such as bone and bone marrow, introduce complications in wet ashing by previously described procedures. In the accompanying detailed procedure, 100% sulphuric acid and 73.60% perchloric acid serve as oxidants with vanadium as catalyst. Reagent preparation, apparatus design, and illustrative reactions are described.
Databáze: OpenAIRE