Synthesis of 3H-1,2-dithiole-3-thiones by a novel oxidative cyclization

Autor:	Thomas J. Curphey, H. Howard Joyner
Rok vydání:	1993
Předmět:	Carbon disulfide Oxidative cyclization Organic Chemistry Oxidative phosphorylation Ring (chemistry) Biochemistry Combinatorial chemistry Catalysis chemistry.chemical_compound chemistry Drug Discovery Acetone Organic chemistry Imidazole
Zdroj:	Tetrahedron Letters. 34:7231-7234
ISSN:	0040-4039
Popis:	Reaction of 3-oxo dithioic acids with a combination of hexamethyldisilathiane and N-chlorosuccinimide in the presence of a catalytic amount of imidazole brings about oxidative ring closure to 3H-1,2-dithiole-3-thiones. Yields vary from poor to good.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::5076d31e230d947c4aaef9fbd39a8c12 https://doi.org/10.1016/s0040-4039(00)79295-1 Zobrazit plný text záznamu