Gas-chromatographic determination of ethylene glycol in serum

Autor:	A Auansakul, W H Porter
Rok vydání:	1982
Předmět:	Detection limit chemistry.chemical_compound Chromatography chemistry Reference values Biochemistry (medical) Clinical Biochemistry Gas chromatography–mass spectrometry Ethylene glycol
Zdroj:	Clinical Chemistry. 28:75-78
ISSN:	1530-8561 0009-9147
DOI:	10.1093/clinchem/28.1.75
Popis:	We describe a new gas-chromatographic procedure for ethylene glycol in serum, determined as the cyclic phenylboronate ester. The method is rapid, requires only 100 microL of serum, and either an OV-1 or an OV-17 column is used. The linear dynamic range extends to at least 5000 mg/L, with a lower limit of detection of 10 mg/L. Analytical recovery of ethylene glycol from serum averaged 97% (95-101%) over the concentration range of 250-5000 mg/L. The method demonstrates good precision, with CVs less than 2.5%, over the concentration range 500-2000 mg/L.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::4f72f8b4c60c58de0f9ca2e76388a28a https://doi.org/10.1093/clinchem/28.1.75 Zobrazit plný text záznamu