ChemInform Abstract: A New, Simple, One-Pot Route for the Synthesis of Azocine Derivatives

Autor:	Mohammad Reza Mohammadizadeh, Maryam Alborz
Rok vydání:	2015
Předmět:	Acenaphthoquinone Addition reaction chemistry.chemical_compound Chemistry Simple (abstract algebra) Proton NMR Organic chemistry Azocine General Medicine Carbon-13 NMR Oxidative cleavage Combinatorial chemistry Intermediate product
Zdroj:	ChemInform. 46
ISSN:	0931-7597
DOI:	10.1002/chin.201517239
Popis:	A novel, simple, one-pot procedure for the synthesis of new 7H-naphtho[1,8-ef]pyrimido[4,5-b]azocine-7,10,12,13(8H,9H,11H)-tetraones by the addition reaction of acenaphthoquinone and 6-aminouracil derivatives followed by oxidative cleavage of the corresponding intermediate product in the presence of lead(IV) acetate is reported. Clean reactions, excellent yields, and mild conditions are the main features of this method. The structural assignments are supported by 1H NMR, 13C NMR, and X-ray crystallography data.
Databáze:	OpenAIRE
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