Synthesis and NMR spectroscopy of stable isotope-labelled phenols and L-tyrosines

Autor:	M. W. M. M. Aarts, F. R. van der Heide, E. G. Buitenhuis, C. Winkel, Johan Lugtenburg
Rok vydání:	2010
Předmět:	chemistry.chemical_compound Chemistry Stable isotope ratio Erwinia herbicola Acetone Organic chemistry Phenol General Chemistry Nuclear magnetic resonance spectroscopy Phenols Carbon-13 NMR
Zdroj:	Recueil des Travaux Chimiques des Pays-Bas. 108:139-146
ISSN:	0165-0513
DOI:	10.1002/recl.19891080405
Popis:	The syntheses of (17O)phenol from (17O)water, (18O)phenol from (18O)water, (1-13C)-phenol and (4-13C)phenol from (2-13C)acetone and (2-13C)phenol and (3-13C)phenol from (1-13C)-acetone with high isotopic enrichment are described. The labelled phenols are converted into their corresponding L-tyrosines by the bacterium Erwinia herbicola. A full analysis of the 1H and 13C NMR spectra of phenol and L-tyrosine is reported.
Databáze:	OpenAIRE
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