Synthesis of Dimethyl Octahydroquinazolinones by using Electrochemically Prepared Copper Oxide Nanoparticles
| Autor: | Bhaskar H. Zaware, Manisha R. Sawant, Anjali S. Rajbhoj, Suresh T. Gaikwad |
|---|---|
| Rok vydání: | 2020 |
| Předmět: |
Copper oxide
chemistry.chemical_element Nanoparticle 02 engineering and technology General Chemistry 010402 general chemistry 021001 nanoscience & nanotechnology Electrochemistry 01 natural sciences Copper 0104 chemical sciences Catalysis chemistry.chemical_compound chemistry Thiourea Yield (chemistry) Fourier transform infrared spectroscopy 0210 nano-technology Nuclear chemistry |
| Zdroj: | Asian Journal of Chemistry. 32:1895-1902 |
| ISSN: | 0975-427X 0970-7077 |
| DOI: | 10.14233/ajchem.2020.22704 |
| Popis: | Present work involves the synthesis of substituted dimethyl octahydroquinazolinones by using electrochemically prepared copper oxide nanoparticles as catalyst in microwave. Copper oxide nanoparticles were prepared in appreciable yield by using electrochemical reduction method of synthesis in the presence of tetrabutylphosphonium bromide for capping. The prepared nanoparticles were analyzed by UV, FTIR, TGA, X-ray diffraction and electron microscopic studies. The nanoparticles of copper oxide then were successfully used as a catalyst in multicomponent reaction between diketones, substituted aldehydes and urea/thiourea to synthesize substituted dimethyl octahydroquinazolinones. |
| Databáze: | OpenAIRE |
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