13C- and 1H-detection under fast MAS for the study of poorly available proteins: application to sub-milligram quantities of a 7 trans-membrane protein

Autor:	Anthony Watts, Krisztina Varga, Lubica Asilmovska, Marc Philipp Pfeil, Peter J. Judge, Victoria A. Higman, Garrick F. Taylor, Hugh R. W. Dannatt
Rok vydání:	2015
Předmět:	biology Resolution (mass spectrometry) Chemistry Analytical chemistry Bacteriorhodopsin Biochemistry Spectral line Membrane protein Solid-state nuclear magnetic resonance Yield (chemistry) Helix biology.protein Magic angle spinning Spectroscopy
Zdroj:	Journal of Biomolecular NMR. 62:17-23
ISSN:	1573-5001 0925-2738
Popis:	We demonstrate that 13C-detected spectra recorded using fast (60 kHz) magic angle spinning on sub-milligram (
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::4b17207a6a0a1a8c13167e1350378c0e https://doi.org/10.1007/s10858-015-9911-1 Zobrazit plný text záznamu Full text from SpringerLink