Synthesis and characterization of nanocrystalline Al0.5Ag0.5TiO3powder
| Autor: | K.V. Prasad, Anal K. Jha, L. K. Sahay, Sandeep Kumar |
|---|---|
| Rok vydání: | 2013 |
| Předmět: |
Fluid Flow and Transfer Processes
Materials science Scanning electron microscope Mechanical Engineering Nucleation Nanoparticle Nanotechnology Atomic and Molecular Physics and Optics Catalysis Nanocrystalline material Electronic Optical and Magnetic Materials Chemical engineering Transmission electron microscopy visual_art Ceramics and Composites visual_art.visual_art_medium Ceramic Electrical and Electronic Engineering Fourier transform infrared spectroscopy Biotechnology Monoclinic crystal system |
| Zdroj: | Advances in nano research. 1:211-218 |
| ISSN: | 2287-237X |
| DOI: | 10.12989/anr.2013.1.4.211 |
| Popis: | A low-cost, green and reproducible citric acid assisted synthesis of nanocrystalline Al0.5Ag0.5TiO3 (n-AAT) powder is reported. X-ray, FTIR, energy dispersive X-ray, transmission electron microscopy and scanning electron microscopy analyses are performed to ascertain the formation of n-AAT. X-ray diffraction data analysis indicated the formation of monoclinic structure. Spherical shaped particles having the sizes of 3-15 nm are found. The mechanism of nano-transformation for the soft-chemical synthesis of n-AAT has been explained using simple organic chemistry rules and nucleation and growth theory. Dielectric study revealed that AAT ceramic might be a suitable candidate for capacitor applications. |
| Databáze: | OpenAIRE |
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