A first 1,2,4-triazole PbII Complex: Thermal, spectroscopic and structural studies, [Pb2(trz)2(CH3COO)(NO2)]n

Autor:	AA Soudi, Sahar Moazzenchi, Ali Morsali
Rok vydání:	2006
Předmět:	Chemistry Coordination polymer Coordination number 1 2 4-Triazole Carbon-13 NMR Inorganic Chemistry Crystallography chemistry.chemical_compound Elemental analysis Materials Chemistry Proton NMR Physical and Theoretical Chemistry Spectroscopy Lone pair
Zdroj:	Inorganic Chemistry Communications. 9:1259-1262
ISSN:	1387-7003
DOI:	10.1016/j.inoche.2006.08.003
Popis:	A 3D Pb II coordination polymer containing 1,2,4-triazole (trz) and two different anions, [Pb 2 (trz) 2 (CH 3 COO)(NO 2 )] n has been synthesized and characterized by elemental analysis, IR-, 1 H NMR-, 13 C NMR spectroscopy and studied by thermal as well as X-ray crystallography. The single-crystal X-ray data shows two types of Pb 2+ -ions with coordination numbers of seven, Pb(1) and Pb(2) with hemidirected and holodirected geometries, respectively.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::437efadd1ba74f504162015f7c2e5ddd https://doi.org/10.1016/j.inoche.2006.08.003 Zobrazit plný text záznamu Full Text from ScienceDirect