Magnetic Behavior of Mechanically Milled FeNi-CoO Nanocomposites

Autor: Sanjay R. Mishra, I. Dubenko, K. Marasinghe, S. Roy, N. Ali, Joseph Losby
Rok vydání: 2004
Předmět:
Zdroj: IEEE Transactions on Magnetics. 40:2716-2720
ISSN: 0018-9464
DOI: 10.1109/tmag.2004.830227
Popis: The effects of crystallite size and ball-mill-induced defects on the magnetic properties of ferromagnetic (FM) FeNi-antiferromagnetic (AFM) CoO (Neel Temperature=290 K) nanocomposites are assessed by magnetic measurements. Asymmetric zero-field-cooled (ZFC) hysteresis loops were observed for samples milled for 30h and longer. The field-cooled (FC) hysteresis loops were asymmetric and shifted in the direction opposite to the cooling field. The enhancement of coercivity and squareness ratio (M/sub R//M/sub S/), along with a presence of a loop shift after field cooling indicates the presence of an exchange bias effect between the FM and AFM phases of the composite. The exchange bias field extracted from the 5 K FC measurement shows continuous enhancement with milling times up to 30 hours and a reduction upon prolonged milling. The temperature dependent exchange bias field measurement shows that the exchange bias field reduces to zero at temperature T
Databáze: OpenAIRE