Sintering behavior, infrared spectra and microwave dielectric characteristics analysis for Ce2Zr3(MoO4)9 ceramics achieved by reaction-sintering method
Autor: | Xu Ying, Yishan Jiang, Haitao Wu, Lintao Liu, Juna Chen, Jialun Du, Wenhong Tao, Xu Zhou |
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Rok vydání: | 2021 |
Předmět: |
Materials science
Scanning electron microscope Rietveld refinement Mechanical Engineering Metals and Alloys Sintering Infrared spectroscopy 02 engineering and technology Dielectric 010402 general chemistry 021001 nanoscience & nanotechnology Microstructure 01 natural sciences 0104 chemical sciences Chemical bond Mechanics of Materials visual_art Materials Chemistry visual_art.visual_art_medium Ceramic Composite material 0210 nano-technology |
Zdroj: | Journal of Alloys and Compounds. 875:160096 |
ISSN: | 0925-8388 |
DOI: | 10.1016/j.jallcom.2021.160096 |
Popis: | Ce2Zr3(MoO4)9 (CZM) ceramics were prepared successfully through the reaction-sintering (RS) method and a single phase was detected in X-ray diffraction patterns. The microstructures of ceramics were observed by a scanning electron microscopy. Based on the results of Rietveld refinement, the influence of chemical bonds parameters on microwave dielectric properties were analyzed by complex chemical bond theory. The lattice vibrational characteristics were investigated by far-infrared reflection spectroscopy. The promising dielectric properties of CZM ceramics were er = 10.1, Q×f = 69,705 GHz and τf = −6.34 ppm/°C, sintered at 850 °C. |
Databáze: | OpenAIRE |
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