Silicon nanochains preparation with hydrothermal synthesis
| Autor: | Y.H. Tang, Yang-Wen Chen, Liang-wu Lin, Chi Guo, L.Z. Pei |
|---|---|
| Rok vydání: | 2007 |
| Předmět: |
Materials science
Silicon Mechanical Engineering chemistry.chemical_element Condensed Matter Physics Microstructure Hydrothermal circulation Crystallography chemistry Chemical engineering Mechanics of Materials Transmission electron microscopy Hydrothermal synthesis General Materials Science Diamond cubic Selected area diffraction High-resolution transmission electron microscopy |
| Zdroj: | Materials Science and Engineering: B. 138:189-192 |
| ISSN: | 0921-5107 |
| DOI: | 10.1016/j.mseb.2006.09.006 |
| Popis: | Silicon nanochains over 1 μm in length and 50–100 nm in diameter have been synthesized by hydrothermal synthesis with silicon powders as start materials and de-ionized water as reaction medium, the growth condition was controlled at 470 °C and 9.7 MPa in a sealed reaction kettle. The morphology and microstructure of the production were characterized by transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), selected area electron diffraction (SAED); the results revealed that the silicon nanochains have diamond structure. Energy dispersive X-ray spectrum (EDS) was used to analyze the composition of the final production and the possible growth mechanism of silicon nanochain under supercritical hydrothermal condition was proposed. |
| Databáze: | OpenAIRE |
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