Separation and quantitation of nitrobenzenes and their reduction products nitroanilines and phenylenediamines by reversed-phase high-performance liquid chromatography

Autor:	Tirumuru V. Reddy, L.W. Chang, F. B. Daniel, Gunda Reddy, Edith L.C. Lin, Matthew Smith, B.E. Wiechman
Rok vydání:	1993
Předmět:	Detection limit Chromatography Dinitrobenzene Organic Chemistry General Medicine Reversed-phase chromatography Biochemistry High-performance liquid chromatography Analytical Chemistry Nitrobenzene chemistry.chemical_compound Aniline chemistry Methanol Triethylamine
Zdroj:	Journal of Chromatography A. 655:331-335
ISSN:	0021-9673
DOI:	10.1016/0021-9673(93)83240-s
Popis:	A reversed-phase high-performance liquid chromatographic method for the separation and quantitation of a mixture consisting of nitrobenzene, dinitrobenzene isomers, 1,3,5-trinitrobenzene and their reduction products: aniline, nitroanilines and phenylenediamines has been developed. The method is sensitive and highly reproducible. The mixture is resolved on a Zorbax C 8 column with 0.1% triethylamine and methanol as the mobile phase. The detection limits for individual chemicals at 254 nm are in the range of 25–50 ng.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::3ec2f23e547f4ae7d2bca190928d4689 https://doi.org/10.1016/0021-9673(93)83240-s Zobrazit plný text záznamu