Efficient Microwave Solvent-Free Synthesis of Flavones, Chromones, Coumarins and Dihydrocoumarins
Autor: | Diego Manuel Ruiz, Gustavo P. Romanelli, Horacio J. Thomas, Juan Carlos Autino, Graciela T. Baronetti, Daniel Oscar Bennardi |
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Rok vydání: | 2008 |
Předmět: | |
Zdroj: | Letters in Organic Chemistry. 5:607-615 |
ISSN: | 1570-1786 |
DOI: | 10.2174/157017808786857570 |
Popis: | Simple, clean, environmentally friendly procedures for the solvent-free preparation of coumarins, dihydrocou- marins, flavones and chromones under microwave heating are described. Silica-supported Wells-Dawson heteropolyacid (H6P2W18O62·24 H2O) was employed as catalyst. High selectivity, very good yields and short reaction times were ob- tained. The results are compared with those of the reactions performed under conventional heating. |
Databáze: | OpenAIRE |
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