Determination of Ciprofloxacin by Flow Injection Analysis Based on Chemiluminescence System

Autor: Shi-lü Chen, Hui-chun Zhao, Zhuoyong Zhang, Xia Li, Baohua Song, Xiaoli Wang
Rok vydání: 2006
Předmět:
Zdroj: Journal of Rare Earths. 24:285-288
ISSN: 1002-0721
Popis: A novel flow injection chemiluminescence (CL) method for the determination of ciprofloxacin (CPLX) was reported. The proposed method is based on luminescence produced by KMnO 4 -Na 2 S 2 O 4 -Tb 3+ -CPLX chemiluminescence (CL) system. The effects of some critical experimental conditions were discussed and the optimization of working conditions was investigated. The linear dynamic range is 3.00×10 −8 ∼9.00×10 −7 mol·L −1 and the detection limit for CPLX is 4.40 × 10 −9 mol·L −1 . This method was applied to the determination of CPLX in tablet, urine, and serum samples and the recoveries of real sample analyses were in the range from 110±4 to 104±4.
Databáze: OpenAIRE