Synthesis and Mesomorphic Investigations of Liquid Crystalline Compounds Having a Benzothiazole Ring
Autor: | B. T. Thaker, N. B. Patel, U. Makawana, B. S. Patel, D. B. Solanki, Y. T. Dhimmar, Kishan Patel, N. J. Chothani |
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Rok vydání: | 2013 |
Předmět: |
Phase transition
Materials science General Chemistry Condensed Matter Physics Mass spectrometry Ring (chemistry) law.invention Crystallography Homologous series chemistry.chemical_compound chemistry Benzothiazole Optical microscope law Liquid crystal Elemental analysis Organic chemistry General Materials Science |
Zdroj: | Molecular Crystals and Liquid Crystals. 575:64-76 |
ISSN: | 1563-5287 1542-1406 |
Popis: | Two homologous series of calamitic liquid crystals containing a benzothiazole ring and two different linkages have been prepared, and their liquid crystalline properties are studied and compared with each other and those of similar structure. The mesogens with only the cinnamate linking group showed better thermal properties than those with an ester. Nematic and smectic phases were observed. All the compounds of both the series were characterized by elemental analysis, FT-IR, mass spectrometry, 1H-NMR, and 13C-NMR. Phase transition temperatures and the thermal parameters were obtained from differential scanning calorimetery (DSC). The textural observations were performed using hot-stage Polarizing Optical Microscopy (POM). |
Databáze: | OpenAIRE |
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