Hydrothermal synthesis of silver nanoparticles in Arabic gum aqueous solutions
Autor: | Wei-ping Gan, Tian-tian Ge, Chao Yang, Jian Zhou, Ying-fen Li, Zhi-qiang Lu |
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Rok vydání: | 2015 |
Předmět: |
Green chemistry
Steric effects Aqueous solution Materials science Metallurgy Metals and Alloys Geotechnical Engineering and Engineering Geology Condensed Matter Physics Hydrothermal circulation Silver nanoparticle Pulmonary surfactant Materials Chemistry Hydrothermal synthesis Fourier transform infrared spectroscopy Nuclear chemistry |
Zdroj: | Transactions of Nonferrous Metals Society of China. 25:2081-2086 |
ISSN: | 1003-6326 |
DOI: | 10.1016/s1003-6326(15)63818-3 |
Popis: | Finely divided silver nanoparticles were synthesized via the hydrothermal method. Arabic gum (AG) was used as both the reductant and steric stabilizer without any other surfactant. By adjusting the reaction temperature, mass ratio of AG to AgNO3, and reaction time, silver nanoparticles with different morphological characteristics could be obtained. The products were characterized by UV–Vis, FTIR, TEM, SEM, and XRD measurements. It was found that temperature and AG played an important role in the synthesis of mono-disperse silver nanoparticles. Well dispersed and quasispherical silver nanoparticles were obtained under the optimal synthesis conditions of 10 mmol/L AgNO3, m(AG)/m(AgNO3)=1:1, 160 °C and 3 h. |
Databáze: | OpenAIRE |
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