Synthesis of 3-Formylbenzenesulfonyl Chloride Derivatives

Autor: Changshun Bao, Xinjie Liang, Zi'ao Liu, Dake Song, Guoliang Chen, Tao Shi, Xuan Zhao, Xuefei Bao
Rok vydání: 2017
Předmět:
Zdroj: Synthesis. 49:3165-3170
ISSN: 1437-210X
0039-7881
DOI: 10.1055/s-0036-1589015
Popis: A synthetic route to 3-formylbenzenesulfonyl chloride derivatives from the corresponding benzaldehydes has been developed. The key step in this procedure is the conversion of aldehyde bisulfite adducts to target compounds via a two-stage reaction in the presence of Na2SO4. A series of 3-formylbenzenesulfonyl chloride derivatives were prepared by this method and identified by chemical derivatization method.
Databáze: OpenAIRE