Synthesis of 3-Formylbenzenesulfonyl Chloride Derivatives
Autor: | Changshun Bao, Xinjie Liang, Zi'ao Liu, Dake Song, Guoliang Chen, Tao Shi, Xuan Zhao, Xuefei Bao |
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Rok vydání: | 2017 |
Předmět: | |
Zdroj: | Synthesis. 49:3165-3170 |
ISSN: | 1437-210X 0039-7881 |
DOI: | 10.1055/s-0036-1589015 |
Popis: | A synthetic route to 3-formylbenzenesulfonyl chloride derivatives from the corresponding benzaldehydes has been developed. The key step in this procedure is the conversion of aldehyde bisulfite adducts to target compounds via a two-stage reaction in the presence of Na2SO4. A series of 3-formylbenzenesulfonyl chloride derivatives were prepared by this method and identified by chemical derivatization method. |
Databáze: | OpenAIRE |
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