OXIDATIVE-ALKALINE DELIGNIFICATION OF WHEAT STRAW

Autor: Pen, R.Z., Shapiro, I.L., Ambrosovich, I.A.
Jazyk: angličtina
Rok vydání: 2021
Předmět:
DOI: 10.34660/inf.2021.82.11.015
Popis: Stalks of straw Triticum sp. delignified with hydrogen peroxide and peracetic acid, followed by alkaline extraction. Conditions of the oxidation stage: initial concentration of acetic acid 36%, hydrogen peroxide 12%, sulfuric acid (catalyst for the formation of peracetic acid) 0.45%; hydronic module 3; temperature 85°C; duration 2 hours. The product obtained with a yield of 85.8% was treated with a sodium hydroxide solution at hydromodule 3 and a temperature of 85°C; the concentration of alkali was changed in the range of 2 ... 4%, duration - 0.5 ... 1.5 hours. The maximum yield of technical cellulose of 40.2% in the absence of "lack of penetration" was obtained at an alkali concentration of 3.6% and a duration of 1.5 hours.
Databáze: OpenAIRE