Comparison of Four Methods for Digesting Food Samples for Determination of Trace Levels of Cadmium by Flameless Atomic Absorption Spectrophotometry

Autor: Genevieve Cassanas, Jean C Cabanis, Marie T Cabanis, Suzanne Brun
Rok vydání: 1988
Předmět:
Zdroj: Journal of AOAC INTERNATIONAL. 71:1033-1037
ISSN: 0004-5756
DOI: 10.1093/jaoac/71.5.1033
Popis: We compared 4 digestion procedures, namely, sulfuric-nitric acid in an open flask, nitric acid under pressure, sulfuric-nitric acid with refluxing, and nitric-hydrochloric-peroxide with refluxing, for the determination of cadmium by flameless atomic absorption spectrophotometry in 3 foodstuffs: rice, beef, and cream cheese. The foodstuffs were homogenized and divided into several batches for analysis. The results were evaluated using a 2-way cross analysis of variance. The study revealed that the digestion procedure was a highly significant factor (P < 10 4) in the analysis of the 3 foods; whereas the nature of the foodstuffs was not significant for rice and meat and only slightly significant (P
Databáze: OpenAIRE