A multiple ion counter total evaporation (MICTE) method for precise analysis of plutonium by thermal ionization mass spectrometry
| Autor: | Azim Kara, Joel R. Maassen, William S. Kinman, Dennis Lopez, J. D. Inglis, Robert E. Steiner |
|---|---|
| Rok vydání: | 2017 |
| Předmět: |
Reproducibility
Isotope Chemistry Health Toxicology and Mutagenesis Nuclear forensics 010401 analytical chemistry Public Health Environmental and Occupational Health Analytical chemistry Evaporation chemistry.chemical_element Thermal ionization mass spectrometry 010403 inorganic & nuclear chemistry 01 natural sciences Pollution 0104 chemical sciences Analytical Chemistry Ion Plutonium Nuclear Energy and Engineering Radiology Nuclear Medicine and imaging Spectroscopy |
| Zdroj: | Journal of Radioanalytical and Nuclear Chemistry. 312:663-673 |
| ISSN: | 1588-2780 0236-5731 |
| DOI: | 10.1007/s10967-017-5259-1 |
| Popis: | This paper presents a total evaporation method for the analysis of sub-picogram quantities of Pu, utilizing an array of multiple ion counters. Data from three standards are presented to assess the utility of the technique. An external precision of 1.5% RSD (2σ) was achieved on aliquots approaching 100 fg for the minor 240Pu isotope. Accurate analysis of |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|