Analysis of mixtures of six carbon unsaturates
Autor: | R. W. Dunning, J. A. Leonard |
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Rok vydání: | 1969 |
Předmět: | |
Zdroj: | Chromatographia. 2:293-297 |
ISSN: | 1612-1112 0009-5893 |
DOI: | 10.1007/bf02258966 |
Popis: | Practical resolution of twelve hexene isomers is described. Total analysis time is forty minutes and separation is effected by means of a 100 metre squalane coated capillary column maintained at 0°C. Details of a technique allowing the rapid determination of the skeletal distribution of these isomers is given. Olefins are hydrogenated via a catalyst-containing liner which is itself part of a modified injection block. Hydrogen is used both as reactant and carrier gas in this process. |
Databáze: | OpenAIRE |
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