Contribution of Microwave to the Formation of Octacalcium Phosphate Intercalating Succinate Ions
| Autor: | Soichiro Yamaguchi, Yoshiaki Tsunawaki, Kiyoko Sakamoto, Toshitaka Idehara, Makoto Asakawa, Seitaro Mitsudo, Yuusuke Yamaguchi |
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| Rok vydání: | 2021 |
| Předmět: |
010302 applied physics
Radiation Materials science Intercalation (chemistry) chemistry.chemical_element Calcium Condensed Matter Physics 01 natural sciences Ion 010309 optics chemistry.chemical_compound chemistry Chemical engineering Succinic acid Reagent 0103 physical sciences Microwave irradiation Electrical and Electronic Engineering Octacalcium phosphate Instrumentation Microwave |
| Zdroj: | Journal of Infrared, Millimeter, and Terahertz Waves. 42:409-415 |
| ISSN: | 1866-6906 1866-6892 |
| DOI: | 10.1007/s10762-021-00774-x |
| Popis: | We applied microwave light with frequencies 10, 212, and 419 GHz to form octacalcium phosphate (OCP) intercalated with succinate ions (SCI). The composition of starting reagents (i.e., α-type tricalcium phosphate (TCP), calcium hydrogenphosphate dihydrate (DCPD), and SCI in pure water) did not enable us to form OCP intercalated with SCI in a thermostatic water bath. Although microwave irradiation typically acts as a heat source in water, it has brought a valuable contribution to OPC formation. This paper reports the following interesting result; microwave irradiation of power less than 0.1 W enabled us to synthesize OCP intercalated with SCI which was not possible to form with power values exceeding 0.1 W. |
| Databáze: | OpenAIRE |
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