Structural characterization of NiO films on Al2O3(0001)

Autor: M. Noblet, Yves Samson, C Mocuta, Antoine Barbier, G Renaud
Rok vydání: 2000
Předmět:
Zdroj: Journal of Magnetism and Magnetic Materials. 211:283-290
ISSN: 0304-8853
Popis: NiO films on clean α-Al2O3(0 0 0 1) were prepared by molecular beam epitaxy. Two parameters were considered: the growth temperature (320–700°C) and the film thickness (29–200 nm). Low energy electron diffraction (LEED) patterns of the deposits show a six-fold symmetry. The samples were ex situ characterized by atomic force microscopy (AFM) and by grazing incidence X-ray diffraction. For all samples, NiO islands with different sizes and shapes were observed. A layer of pyramidal NiO islands, with triangular facets is present. Depending on the sample, also hexagonal or square islands were observed. The angles of the triangular facets correspond to (1 0 0) surfaces of the NiO(1 1 1). X-ray diffraction evidences that the NiO film grows with the (1 1 1) plane parallel to the (0 0 0 1)Al2O3 one. Twinned and not-twinned face centered cubic (FCC) NiO(1 1 1) stacking are present in approximately equal quantities. The crystallographic quality of the NiO layers was investigated.
Databáze: OpenAIRE