CuI Crystal Growth in Acetonitrile Solvent by the Cycle-Evaporation Method

Autor:	Jianguo Pan, Xing Li, Shuying Yang, Yuebao Li, Yuejie Cui, Lei Han
Rok vydání:	2009
Předmět:	Inorganic chemistry Analytical chemistry Evaporation Crystal growth General Chemistry Condensed Matter Physics Solvent Crystal Thermogravimetry chemistry.chemical_compound chemistry Differential thermal analysis General Materials Science Acetonitrile Powder diffraction
Zdroj:	Crystal Growth & Design. 9:3825-3827
ISSN:	1528-7505 1528-7483
DOI:	10.1021/cg900775a
Popis:	Acetonitrile solvent was applied to grow CuI crystals by the cycle-evaporation method with Cu as the reductant. The growth temperature was 70 °C. The process was performed in a nitrogen atmosphere. Clear, millimeter-scaled CuI single crystals were obtained. Moreover, UV−visible spectra, IR spectra, and XRD were used to investigate the redox processes in the solution. The crystal was characterized by X-ray powder diffraction and differential thermal /thermogravimetry analysis.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::36796cc6b3765fcb4d182f177acb5b92 https://doi.org/10.1021/cg900775a Zobrazit plný text záznamu