Determination of hydrazine in polyvinylpyrrolidone by derivatization and square wave voltammetry

Autor:	Regina Colonnese, Robert M. Ianniello
Rok vydání:	1989
Předmět:	Polyvinylpyrrolidone Drop (liquid) Analytical chemistry Square wave Analytical Chemistry Azine chemistry.chemical_compound Salicylaldehyde chemistry Electrode medicine Derivatization Voltammetry medicine.drug Nuclear chemistry
Zdroj:	Mikrochimica Acta. 98:7-14
ISSN:	1436-5073 0026-3672
Popis:	A rapid and precise method has been developed for the determination of hydrazine in polyvinylpyrrolidone (PVP). Hydrazine is converted to salicylaldazine by reaction with salicylaldehyde. After extraction, the azine is reduced at −1.56 V versus the SCE at the hanging drop electrode. Detection is accomplished using square wave voltammetry and comparison to an external salicylaldazine standard. The described procedure can detect as little as 70 ng/g hydrazine in PVP.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::357c4a461e5bf0ce9ed85eb55406e277 https://doi.org/10.1007/bf01244511 Zobrazit plný text záznamu Full text from SpringerLink