Rapid determination of 226Ra in emergency urine samples
Autor: | Brian K. Culligan, Robin C. Utsey, Sherrod L. Maxwell, Daniel R. McAlister, Jay B. Hutchison |
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Rok vydání: | 2014 |
Předmět: |
Chromatography
Alpha spectrometry Health Toxicology and Mutagenesis Sample (material) Public Health Environmental and Occupational Health Urine Pollution Analytical Chemistry Nuclear Energy and Engineering Environmental chemistry Environmental science Radiology Nuclear Medicine and imaging Sample preparation National laboratory Spectroscopy |
Zdroj: | Journal of Radioanalytical and Nuclear Chemistry. 300:1159-1166 |
ISSN: | 1588-2780 0236-5731 |
DOI: | 10.1007/s10967-014-3046-9 |
Popis: | A new method has been developed at the Savannah River National Laboratory (SRNL) that can be used for the rapid determination of 226Ra in emergency urine samples following a radiological incident. If a radiological dispersive device event or a nuclear accident occurs, there will be an urgent need for rapid analyses of radionuclides in urine samples to ensure the safety of the public. Large numbers of urine samples will have to be analyzed very quickly. This new SRNL method was applied to 100 mL urine aliquots, however this method can be applied to smaller or larger sample aliquots as needed. The method was optimized for rapid turnaround times; urine samples may be prepared for counting in 90 %), and removes interferences effectively. The sample preparation method can also be adapted to ICP-MS measurement of 226Ra, with rapid removal of isobaric interferences. |
Databáze: | OpenAIRE |
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