Reactions of Carbonyl-Conjugated Alkynes with N-Bromosuccinimide and N-Iodosuccinimide in DMF/H2O and Methanol/Sulfuric Acid: Syntheses of Dihalo Diketones, Dihalo Ketoesters, and Dihalo Acetals†

Autor: Charles L. Kissel, Jason M. Cox, Dale F. Shellhamer, David J. Hill, Victor L. Heasley, Alfred E. Chappell, Cyndi C. Eden, Shanna L. McGovern
Rok vydání: 1998
Předmět:
Zdroj: The Journal of Organic Chemistry. 63:4433-4437
ISSN: 1520-6904
0022-3263
DOI: 10.1021/jo980260n
Popis: The following terminal, carbonyl-conjugated alkynes were reacted with N-bromosuccinimide (NBS) and N-iodosuccinimide (NIS) in MeOH/H2SO4 to give dibromo and diiodo acetals in the indicated yields: ...
Databáze: OpenAIRE