Reactions of Carbonyl-Conjugated Alkynes with N-Bromosuccinimide and N-Iodosuccinimide in DMF/H2O and Methanol/Sulfuric Acid: Syntheses of Dihalo Diketones, Dihalo Ketoesters, and Dihalo Acetals†
Autor: | Charles L. Kissel, Jason M. Cox, Dale F. Shellhamer, David J. Hill, Victor L. Heasley, Alfred E. Chappell, Cyndi C. Eden, Shanna L. McGovern |
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Rok vydání: | 1998 |
Předmět: | |
Zdroj: | The Journal of Organic Chemistry. 63:4433-4437 |
ISSN: | 1520-6904 0022-3263 |
DOI: | 10.1021/jo980260n |
Popis: | The following terminal, carbonyl-conjugated alkynes were reacted with N-bromosuccinimide (NBS) and N-iodosuccinimide (NIS) in MeOH/H2SO4 to give dibromo and diiodo acetals in the indicated yields: ... |
Databáze: | OpenAIRE |
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