Synthesis of Ni-TiN/Si3N4 nanocomposite layers using the electrodeposition method
| Autor: | Esmar Budi, Hadi Nasbey, Leli Kusumawati, Iwan Sugihartono, Widyaningrum Indrasari, Teguh Budi Prayitno |
|---|---|
| Rok vydání: | 2021 |
| Předmět: | |
| Zdroj: | IOP Conference Series: Materials Science and Engineering. 1098:062042 |
| ISSN: | 1757-899X 1757-8981 |
| DOI: | 10.1088/1757-899x/1098/6/062042 |
| Popis: | In an effort to find the best technique for coating metals, the synthesis of the Ni-TiN/Si3N4 nanocomposite layers was carried out. The coating process is carried out using the electrodeposition method. In the electrodeposition process, tungsten carbide (WC) is used as the working electrode. The WC is immersed in the electrolytic solution and is electrified for 5 mA for 15 minutes. During the deposition process, the temperature of the solution is maintained at 35 °C using a hot disc. The crystal structure and phase changes formed in the WC are characterized using X-ray diffraction (XRD). The surface morphology of the layer is investigated by scanning electron microscopy (SEM). Based on the results of the characterization, the size of the Ni-TiN crystal is approximately 488.91 Å. The Si3N4 phase is not detected because it is amorphous. The thickness of the layer formed is approximately 805 nm. This simple technique can be used to produce nanocomposite coatings useful for protecting metals from corrosion. |
| Databáze: | OpenAIRE |
| Externí odkaz: |
|