ChemInform Abstract: Synthesis of Quinolyl-Substituted 4,7-Phenanthrolines
Autor: | K. N. Gusak, V. A. Serzhanina, N. S. Kozlov |
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Rok vydání: | 2010 |
Předmět: | |
Zdroj: | ChemInform. 22 |
ISSN: | 0931-7597 |
DOI: | 10.1002/chin.199112233 |
Popis: | 1-(2-Quinolyl)-3-aryl-4,7-phenanthrolines were synthesized by reacting arylidene-6-quinolylamines with 2-acetylqidnoline in n-butanol in the presence of hydrochloric acid. It was found that the formation of the 4,7-phenanthroline ring is preceded by the stage of formation of an intermediate aminoketone, 1-(2-quinolyl)-3-phenyl-3-(6-quinolylamino)propan-1-one. The IR, UV, PMR, and mass spectra of the synthesized compounds are discussed. |
Databáze: | OpenAIRE |
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