ChemInform Abstract: Synthesis of Quinolyl-Substituted 4,7-Phenanthrolines

Autor: K. N. Gusak, V. A. Serzhanina, N. S. Kozlov
Rok vydání: 2010
Předmět:
Zdroj: ChemInform. 22
ISSN: 0931-7597
DOI: 10.1002/chin.199112233
Popis: 1-(2-Quinolyl)-3-aryl-4,7-phenanthrolines were synthesized by reacting arylidene-6-quinolylamines with 2-acetylqidnoline in n-butanol in the presence of hydrochloric acid. It was found that the formation of the 4,7-phenanthroline ring is preceded by the stage of formation of an intermediate aminoketone, 1-(2-quinolyl)-3-phenyl-3-(6-quinolylamino)propan-1-one. The IR, UV, PMR, and mass spectra of the synthesized compounds are discussed.
Databáze: OpenAIRE