An improved procedure for packing capillaries for capillary electrochromatography

Autor:	B. Lumley, T. M. Khong, David Perrett
Rok vydání:	2001
Předmět:	Solvent system Capillary electrochromatography Chromatography Capillary inlet Capillary action Chemistry Organic Chemistry Clinical Biochemistry Analytical chemistry Biochemistry Analytical Chemistry Electrochromatography Agglomerate High pressure Slurry
Zdroj:	Chromatographia. 54:625-628
ISSN:	1612-1112 0009-5893
DOI:	10.1007/bf02492189
Popis:	This paper introduces a novel improvement to high pressure slurry packing of CEC capillaries. Slurry homogeneity is maintained by constantly stirring in a ‘balanced density’ solvent system in a vessel with a configuration that prevents silica agglomerates from blocking the capillary inlet. Up to nine, one metre length capillaries may be packed simultaneously and repeatably in under 3 hours. All capillaries produced peak efficiencies greater than 100,000 plates/metre with 5 μm Spherisorb ODS1 and showed capillary to capillary variability of less than 10% in terms of peak symmetry and peak efficiency. The data has been presented in part, at the 23rd International Symposium in Chromatography 2000.
Databáze:	OpenAIRE
Externí odkaz:	https://explore.openaire.eu/search/publication?articleId=doi_________::30da362d44d4025be04baf96fb4d6b7f https://doi.org/10.1007/bf02492189 Zobrazit plný text záznamu Full text from SpringerLink