Synthesis of ammonium [14C]thiocyanate

Autor: S. P. Patil, N. Sivaprasad, D. B. Kalgutkar, V. K. P. Unny
Rok vydání: 2003
Předmět:
Zdroj: Journal of Radioanalytical and Nuclear Chemistry. 258:453-455
ISSN: 0236-5731
DOI: 10.1023/b:jrnc.0000011737.68478.c1
Popis: Ammonium [14C]thiocyanate was prepared from potassium [14C]cyanide with a radiochemical yield of 90%. [14C]hydrocyanic acid, generated from potassium [14C]cyanide by sulphuric acid, reacts with aqueous ammonia and elemental sulphur in the presence of trace amounts of ammonium sulphide to yield ammonium [14C]thiocyanate.
Databáze: OpenAIRE