Organophosphorus compounds. Part V: The resolution of O -alkyl hydrogen methylphosphonothioates with (+)- and (−)-α-phenylethylamine

Autor:	H. L. Boter, D. H. J. M. Platenburg
Rok vydání:	1967
Předmět:	chemistry.chemical_classification chemistry Resolution (mass spectrometry) Hydrogen Organic chemistry chemistry.chemical_element General Chemistry Enantiomer Alkyl
Zdroj:	Recueil des Travaux Chimiques des Pays-Bas. 86:399-404
ISSN:	0165-0513
DOI:	10.1002/recl.19670860408
Popis:	A series of four O-alkyl hydrogen methylphosphonothioates, (RO)MeP(S)OH, was resolved using both (+)- and (−)-α-phenylethylamine. Because it gives better results, is rapid and of general applicability the method is to be preferred to that in which alkaloids are used as resolving bases. In one case optical purities of the isolated enantiomers were determined after conversion into acetylcholinesterase inhibitors.
Databáze:	OpenAIRE
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